1,3-BIS(DI-T-BUTYLPHOSPHINOMETHYL)BENZENE synthesis
- Product Name:1,3-BIS(DI-T-BUTYLPHOSPHINOMETHYL)BENZENE
- CAS Number:149968-36-5
- Molecular formula:C24H44P2
- Molecular Weight:394.55
13716-10-4
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$22.00/1 g
626-15-3
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$10.00/1g
149968-36-5
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$47.00/100mg
Yield: 76%
Reaction Conditions:
Stage #1:di(tert-butyl)chlorophosphine;1,3-bis-(bromomethyl)benzene in acetonitrile at 100; for 15 h;Inert atmosphere;
Stage #2: with magnesium in acetonitrile at 0 - 20;Inert atmosphere;
References:
Shih, Wei-Chun;Ozerov, Oleg V. [Organometallics,2015,vol. 34,# 18,p. 4591 - 4597] Location in patent:supporting information