1-(3-methyl-1-benzofuran-2-yl)ethan-1-ol synthesis
- Product Name:1-(3-methyl-1-benzofuran-2-yl)ethan-1-ol
- CAS Number:1158018-33-7
- Molecular formula:C11H12O2
- Molecular Weight:176.21
676-58-4
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Yield:1158018-33-7 93%
Reaction Conditions:
Stage #1: methylmagnesium chloride;3-methylbenzofuran-2-carboxaldehyde in tetrahydrofuran; for 1 h;
Stage #2: with water in tetrahydrofuran;
References:
Schevenels, Florian;Marko, Istvan E. [Organic Letters,2012,vol. 14,# 5,p. 1298 - 1301] Location in patent:supporting information; experimental part
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