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ChemicalBook CAS DataBase List 1-(3-NITROPHENYLSULFONYL)PIPERIDINE

1-(3-NITROPHENYLSULFONYL)PIPERIDINE synthesis

4synthesis methods
-

Yield:91619-31-7 84%

Reaction Conditions:

Stage #1: pyridinium paratoluene sulfonic acidwith trifluoromethanesulfonic acid anhydride;Triphenylphosphine oxide in dichloromethane;
Stage #2: piperidinewith triethylamine in dichloromethane at 0 - 20;

References:

Caddick, Stephen;Wilden, Jonathan D.;Judd, Duncan B. [Journal of the American Chemical Society,2004,vol. 126,# 4,p. 1024 - 1025]

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