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ChemicalBook CAS DataBase List 1,4,7,10,13-PENTAOXA-16-AZACYCLOOCTADECANE

1,4,7,10,13-PENTAOXA-16-AZACYCLOOCTADECANE synthesis

13synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 96 percent / aq. KOH / tetrahydrofuran / 10 h / 0 - 20 °C
2: 24 percent / sodium tert-butoxide / 2-methyl-propan-2-ol; dioxane / 1 h / 20 - 40 °C

References:

Fallouh;Bernier;Virieux;Cristau;Pirat [Phosphorus, Sulfur and Silicon and the Related Elements,2006,vol. 181,# 1,p. 219 - 225]

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