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ChemicalBook CAS DataBase List 1,4-DICYANO-2,3-DIMETHYLBENZENE
103754-49-0

1,4-DICYANO-2,3-DIMETHYLBENZENE synthesis

3synthesis methods
22364-25-6 Synthesis
4-BROMO-2,3-DIMETHYLANILINE

22364-25-6
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1,4-DICYANO-2,3-DIMETHYLBENZENE

103754-49-0
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-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 1.) 48percent aq. HBr, aq. NaNO2, 2.) 48percent aq. HBr, CuBr / 2.) reflux, 30 min
2: 57 percent / dimethylformamide / 4 h / Heating

References:

Lai, Yee-Hing;Yap, Angeline Hui-Tin [Journal of the Chemical Society. Perkin transactions II,1993,# 7,p. 1373 - 1377]

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