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ChemicalBook CAS DataBase List 1,8-Diiodoanthracene
189105-78-0

1,8-Diiodoanthracene synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 1) NaBH4, 2) HCl / 1) MeOH, room temperature, 75 min, 2) MeH, H2O, reflux, 60 min
2: 1) NaBH4, 2) CH3CO2H, HCl / 1) diglyme, MeOH, room temperature, overnight, 2) diglyme, MeOH, room temperature, 60 min

References:

Lovell, James M.;Joule, John A. [Synthetic Communications,1997,vol. 27,# 7,p. 1209 - 1215]