ChemicalBook CAS DataBase List 1-Chloro-N,N,2-trimethylpropenylamine

1-Chloro-N,N,2-trimethylpropenylamine synthesis

2synthesis methods

Product Name:1-Chloro-N,N,2-trimethylpropenylamine
CAS Number:26189-59-3
Molecular formula:C6H12ClN
Molecular Weight:133.62

1-chloro-N,N,2-trimethylpropenylamine is conveniently prepared by the reaction of N,N,2- trimethylpropanamide with Phosgene followed by dehydrochlorination of the intermediate α-chloroiminium chloride (eq 1).^[1,2] Recent unpublished results of our laboratory have shown that Phosphorus Oxychloride or dior triphosgene can also be used for the preparation of TMCE.
1-Chloro-N,N,2-trimethylpropenylamine synthesis

1-Chloro-N,N,2-trimethylpropenylamine synthesis

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: oxalyl dichloride / pentane / -78 - 23 °C / Inert atmosphere
2: trimethylamine / pentane / -78 - 4 °C

References:

O'Brien, Jeannette M.;Kingsbury, Jason S. [Journal of Organic Chemistry,2011,vol. 76,# 6,p. 1662 - 1672]

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1-chlor-N,N,2-trimethylpropaniminium-chlorid

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26189-59-3
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References

1-Chloro-N,N,2-trimethylpropenylamine Related Search:

Epichlorohydrin Methacrylamide N,N'-Methylenebisacrylamide 2-METHYL-2-PROPENE-1-SULFONIC ACID SODIUM SALT Hexamethylphosphoramide

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