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ChemicalBook CAS DataBase List 1-[(chloromethoxy)methyl]-4-methoxybenzene
88023-78-3

1-[(chloromethoxy)methyl]-4-methoxybenzene synthesis

3synthesis methods
1-[(Chloromethoxy)methyl]-4-methoxybenzene is easily prepared from the MTM ether of p-methoxybenzyl alcohol by treatment with  Sulfuryl Chloride in CH2Cl2 at -78 °C followed by solvent evaporation and distillation.
88023-83-0 Synthesis
Benzene, 1-Methoxy-4-[[(Methylthio)Methoxy]Methyl]-

88023-83-0
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Yield:88023-78-3 80%

Reaction Conditions:

with acetyl chloride in dichloromethane;Inert atmosphere;

References:

Anketell, Matthew J.;Paterson, Ian;Sharrock, Theodore M. [Organic and Biomolecular Chemistry,2020,vol. 18,# 40,p. 8109 - 8118] Location in patent:supporting information