1-Cyclopropyl-6,7,8-trifluoro-1,4-dihydro-4-oxoq synthesis
- Product Name:1-Cyclopropyl-6,7,8-trifluoro-1,4-dihydro-4-oxoq
- CAS Number:94695-52-0
- Molecular formula:C13H8F3NO3
- Molecular Weight:283.2
94695-48-4
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94695-52-0
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: tetrahydrofuran / 0.75 h / -78 °C
2: 1.) Ac2O / 1.) 150 deg C, 2 h, 2.) t-BuOH, 10 deg C, 30 min; 45 deg C, overnoght
3: t-BuOK / 2-methyl-propan-2-ol / 18 h / 50 °C
4: HCl / acetic acid / 2 h / 100 °C
References:
Domagala, John M.;Heifetz, Carl L.;Hutt, Marland P.;Mich, Thomas F.;Nichols, Jeffry B.;et al. [Journal of Medicinal Chemistry,1988,vol. 31,# 5,p. 991 - 1001]
94242-51-0
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94695-52-0
89 suppliers
$7.00/250mg
7664-93-9
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94242-51-0
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94695-52-0
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$7.00/250mg
94695-50-8
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94695-52-0
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$7.00/250mg
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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94695-52-0
89 suppliers
$7.00/250mg