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ChemicalBook CAS DataBase List 1-(DIMETHYLAMINO)ISOPROPYLAMINE

1-(DIMETHYLAMINO)ISOPROPYLAMINE synthesis

2synthesis methods
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Yield:108-15-6 93 %Chromat.

Reaction Conditions:

with dodecacarbonyl-triangulo-triruthenium;ammonia;N–phenyl–2–(dicyclohexylphosphino)pyrrole in tert-Amyl alcohol at 150; for 20 h;Cooling with dry ice;Molecular sieve;chemoselective reaction;

References:

Imm, Sebastian;Neubert, Lorenz;Neumann, Helfried;Beller, Matthias [Angewandte Chemie - International Edition,2010,vol. 49,# 44,p. 8126 - 8129] Location in patent:supporting information; experimental part

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