1-Ethyl-2-methylpyrrolidine synthesis
- Product Name:1-Ethyl-2-methylpyrrolidine
- CAS Number:765-79-7
- Molecular formula:C7H15N
- Molecular Weight:113.2
Yield:765-79-7 0.8 mol
Reaction Conditions:
in diethyl ether at 60; for 24 h;Inert atmosphere;Sealed tube;
Steps:
3
Ar atmosphere, 200 mL of dry diethyl ether, 10.00 mol of 2-methylpyrrolidine and 1.00 mol of iodoethyl were placed in a pressure-resistant container made of PFA, sealed and reacted at 60 ° C. for 24 hours .The solution after the reaction was distilled under reduced pressure to obtain 0.800 mol of 1-ethyl-2-methylpyrrolidine.
References:
JP2017/178792,2017,A Location in patent:Paragraph 0058
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