1-ETHYL-3,4-DIHYDRO-ISOQUINOLINE synthesis

5synthesis methods

Product Name:1-ETHYL-3,4-DIHYDRO-ISOQUINOLINE
CAS Number:41173-70-0
Molecular formula:C11H13N
Molecular Weight:159.23

79-03-8 Synthesis

79-03-8
403 suppliers
$9.00/1g

64-04-0
8 suppliers
$10.00/5mL

41173-70-0
19 suppliers
$51.00/100mg

Yield:41173-70-0 96%

Reaction Conditions:

Stage #1: propionyl chloride;phenethylaminewith triethylamine in dichloromethane at 20; for 2 h;Inert atmosphere;
Stage #2: with trichlorophosphate in para-xylene at 20; for 16 h;Inert atmosphere;

References:

Ullrich, Patrick;Schlamkow, Max A.;Choi, Ching-Yi;Kerkenpa?, Hannah;Hen?en, Birgit;Pietruszka, J?rg [European Journal of Organic Chemistry,2021,vol. 2021,# 46,p. 6254 - 6257] Location in patent:supporting information