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ChemicalBook CAS DataBase List 1-ETHYNYL-3,5-DIMETHYL-BENZENE

1-ETHYNYL-3,5-DIMETHYL-BENZENE synthesis

6synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: triphenylphosphine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere
1.2: 3 h / 0 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

References:

Zhu, Xiaotao;Ye, Changqing;Li, Yajun;Bao, Hongli [Chemistry - A European Journal,2017,vol. 23,# 43,p. 10254 - 10258]

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