1-Iodo-2,4-diMethyl-6-nitrobenzene synthesis

1synthesis methods

Yield:593255-20-0 69%

Reaction Conditions:

Stage #1: 2,4-Dimethyl-6-nitroanilinwith sulfuric acid;sodium nitrite in acetic acid at 15 - 75;
Stage #2: with urea;potassium iodide

References:

Liang, Yuxue;Gao, Shuang;Wan, Huihui;Wang, Junwei;Chen, Huilin;Zheng, Zhuo;Hu, Xinquan [Tetrahedron Asymmetry,2003,vol. 14,# 10,p. 1267 - 1273]

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