1-METHYL-4-PHENYL-1H-QUINOLIN-2-ONE synthesis
10synthesis methods
- Product Name:1-METHYL-4-PHENYL-1H-QUINOLIN-2-ONE
- CAS Number:2584-37-4
- Molecular formula:C16H13NO
- Molecular Weight:235.28
![2(1H)-Quinolinone, 1-methyl-4-[[(4-methylphenyl)sulfonyl]oxy]-](/CAS/20200515/GIF/110229-40-8.gif)
Yield:2584-37-4 93%
Reaction Conditions:
with potassium phosphate;2-[2-(dicyclohexylphosphino)-phenyl]-1-methyl-1H-indole;palladium diacetate;triethylamine in tert-butyl alcohol at 50; for 2 h;Inert atmosphere;Suzuki coupling;
References:
Wong, Pui Yu;Chow, Wing Kin;Chung, Kin Ho;So, Chau Ming;Lau, Chak Po;Kwong, Fuk Yee [Chemical Communications,2011,vol. 47,# 29,p. 8328 - 8330] Location in patent:supporting information; experimental part
