1-phenyl-4-(trimethylsilyl)but-3-yn-2-ol synthesis
- Product Name:1-phenyl-4-(trimethylsilyl)but-3-yn-2-ol
- CAS Number:61077-69-8
- Molecular formula:C13H18OSi
- Molecular Weight:218.37
Yield:61077-69-8 92%
Reaction Conditions:
Stage #1: trimethylsilylacetylenewith n-butyllithium in tetrahydrofuran at -78; for 0.25 h;
Stage #2: phenylacetaldehyde in tetrahydrofuran at -78; for 0.5 h;Further stages.;
References:
Lopez, Fernando;Castedo, Luis;Mascarenas, Jose L. [Journal of the American Chemical Society,2002,vol. 124,# 16,p. 4218 - 4219]
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