1-(TERT-BUTOXYCARBONYL)AZETIDINE synthesis
- Product Name:1-(TERT-BUTOXYCARBONYL)AZETIDINE
- CAS Number:147621-21-4
- Molecular formula:C8H15NO2
- Molecular Weight:157.21
254454-54-1
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147621-21-4
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$52.00/100mg
Yield: 86%
Reaction Conditions:
with bismuth(III) oxide;N-ethyl-N,N-diisopropylamine;para-thiocresol in dichloromethaneIrradiation;
Steps:
9 Example 9
a), iodo compound 9 (30mg),Bismuth oxide (2.5mg, 5mol%),P-methylthiophenol (39.4 mg, 3 equiv) was weighed into a 5 mL reaction flask.Then add dichloromethane (1ml)And N,N-diisopropylethylamine (55.4 μL, 3 equiv),Reacted under 1W blue LED light,The reaction was terminated after the iodo compound 9 was consumed.Rotating to remove the reaction solvent and volatile substances,Purification by column chromatography gave Compound 9a (14.3 mg, 86%).
References:
Huazhong University of Science and Technology;Wan Qian;Zeng Jing;Wang Hao;Meng Lingkui;Zhao Xiang;Chen Wei;Tao Jinyi;Shu Penghua CN109265499, 2019, A Location in patent:Paragraph 0119; 0120; 0121
503-29-7
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24424-99-5
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147621-21-4
45 suppliers
$52.00/100mg
503-29-7
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34619-03-9
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147621-21-4
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$52.00/100mg
24424-99-5
863 suppliers
$13.50/25G
147621-21-4
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$52.00/100mg
141699-58-3
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$6.00/250mg
147621-21-4
45 suppliers
$52.00/100mg