10-broMoanthracene-9-carboxylic acid synthesis
- Product Name:10-broMoanthracene-9-carboxylic acid
- CAS Number:6929-81-3
- Molecular formula:C15H9BrO2
- Molecular Weight:301.13
723-62-6
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6929-81-3
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Yield: 90%
Reaction Conditions:
with bromine;acetic acid at 60; for 4 h;
Steps:
1
9-anthracenecarboxylic acid (7.40 g, 3.33 mmol), acetic acid (AcOH, 0.6 L), bromine (Br 2, 1.8 ml) were placed in a reaction vessel and stirred at 60 ° C. for 4 hours for reaction .After completion of the reaction, the reaction product was added to 1.0 L of water saturated with potassium carbonate (K 2 CO 3) and stirred. The resulting solution was neutralized with concentrated hydrochloric acid with sufficient stirring to give a bright yellow precipitate. While thoroughly washing the precipitate with water, it was collected by filtration and dried under reduced pressure to obtain yellow powder 1 (10-bromoanthracene-9-carboxylic acid, 9.0 g) (yield: 90%).
References:
TOYOTA CENTRAL R&D LABS INCORPORATED;MOTEGI, HIROFUMI;SHICHI, AKIRA;MUKAE, YUSUKE;IDOTA, YOSHINORI JP2016/222632, 2016, A Location in patent:Paragraph 0035-0037
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523-27-3
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$6.00/5g
6929-81-3
29 suppliers
$70.00/250mg
523-27-3
396 suppliers
$6.00/5g
6929-81-3
29 suppliers
$70.00/250mg
723-62-6
329 suppliers
$6.00/100mg
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1000210-73-0
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523-27-3
396 suppliers
$6.00/5g
6929-81-3
29 suppliers
$70.00/250mg