Ethanone, 1-(3-pyridinyl)-, O-(phenylMethyl)oxiMe, (1E)- synthesis
- Product Name:Ethanone, 1-(3-pyridinyl)-, O-(phenylMethyl)oxiMe, (1E)-
- CAS Number:1010079-98-7
- Molecular formula:C14H14N2O
- Molecular Weight:226.27
Yield:1010079-98-7 99%
Reaction Conditions:
Stage #1: (E)-1-(pyridin-3-yl)ethanone oximewith sodium hydride in N,N-dimethyl-formamide;mineral oil at -15 - -10; for 0.75 h;Inert atmosphere;
Stage #2: benzyl bromide in N,N-dimethyl-formamide;mineral oil at -12 - -10;Inert atmosphere;
References:
Huang, Kun;Ortiz-Marciales, Margarita;Hughes, David [Organic Syntheses,2010,vol. 87,p. 36 - 52] Location in patent:experimental part
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