BENZYL N-[(3S,4R)-3-FLUOROPIPERIDIN-4-YL]CARBAMATE HCL synthesis

3synthesis methods

Product Name:BENZYL N-[(3S,4R)-3-FLUOROPIPERIDIN-4-YL]CARBAMATE HCL
CAS Number:1034057-93-6
Molecular formula:C13H18ClFN2O2
Molecular Weight:288.75

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BENZYL N-[(3S,4R)-3-FLUOROPIPERIDIN-4-YL]CARBAMATE HCL

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: sodium carbonate / 1,4-dioxane / 0.25 h / 0 °C
2: hydrogenchloride / 1,4-dioxane; dichloromethane / 4 h / 0 - 20 °C

References:

Reck, Folkert;Alm, Richard A.;Brassil, Patrick;Newman, Joseph V.;Ciaccio, Paul;McNulty, John;Barthlow, Herbert;Goteti, Kosalaram;Breen, John;Comita-Prevoir, Janelle;Cronin, Mark;Ehmann, David E.;Geng, Bolin;Godfrey, Andrew Aydon;Fisher, Stewart L. [Journal of Medicinal Chemistry,2012,vol. 55,# 15,p. 6916 - 6933]

1-Piperidinecarboxylic acid, 3-fluoro-4-[[(phenylmethoxy)carbonyl]amino]-, 1,1-dimethylethyl ester, (3S,4R)-

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References

907544-20-1 Synthesis

tert-butyl (3S,4R)-4-aMino-3-fluoropiperidine-1-carboxylate

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References

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