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1035229-33-4

5-(benzyloxy)-8-(2-chloroacetyl)-2H-benzo[b][1,4]oxazin-3(4H)-one synthesis

5synthesis methods
1035229-32-3 Synthesis
8-acetyl-5-(benzyloxy)-2H-benzo[b][1,4]oxazin-3(4H)-one

1035229-32-3
34 suppliers
$35.00/100mg

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Yield:1035229-33-4 94%

Reaction Conditions:

with N,N,N-trimethylbenzenemethanaminium dichloroiodate in dichloromethane;water;acetic acid at 65; for 20 h;Inert atmosphere;

References:

Sweis, Ramzi F.;Wang, Zhi;Algire, Mikkel;Arrowsmith, Cheryl H.;Brown, Peter J.;Chiang, Gary G.;Guo, Jun;Jakob, Clarissa G.;Kennedy, Steven;Li, Fengling;Maag, David;Shaw, Bailin;Soni, Nirupama B.;Vedadi, Masoud;Pappano, William N. [ACS Medicinal Chemistry Letters,2015,vol. 6,# 6,p. 695 - 700] Location in patent:supporting information

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