5-Benzyl-10-oxo-10,11-dihydro-5H-dibenz[b,f]azepine synthesis
- Product Name:5-Benzyl-10-oxo-10,11-dihydro-5H-dibenz[b,f]azepine
- CAS Number:10464-31-0
- Molecular formula:C21H17NO
- Molecular Weight:299.37
76041-86-6
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$87.00/100 mg
10464-31-0
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$125.00/2 mg
Yield:-
Steps:
Multi-step reaction with 3 steps
1: 88 percent / NaOtBu / Pd(OAc)2; rac-BINAP / toluene
2: 97 percent / NaH / dimethylformamide
3: 86 percent / LDA; TMEDA; n-BuLi / tetrahydrofuran; hexane / 4 h / -20 °C
References:
Lohse, Olivier;Beutler, Ulrich;Fünfschilling, Peter;Furet, Pascal;France, Julien;Kaufmann, Daniel;Penn, Gerhard;Zaugg, Werner [Tetrahedron Letters,2001,vol. 42,# 3,p. 385 - 389]
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332081-60-4
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10464-31-0
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1027035-99-9
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10464-31-0
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2042-37-7
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$7.00/10g
10464-31-0
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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10464-31-0
16 suppliers
$125.00/2 mg