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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
104940-65-0

1-(6-Chloro-9H-purin-9-yl)-1-deoxy-2,3-O-isopropylidene-beta-D-ribofuranuronoyl chloride synthesis

3synthesis methods
2140-11-6 Synthesis
2',3'-O-Isopropylideneinosine

2140-11-6
141 suppliers
$8.00/1g

1-(6-Chloro-9H-purin-9-yl)-1-deoxy-2,3-O-isopropylidene-beta-D-ribofuranuronoyl chloride

104940-65-0
17 suppliers
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 83 percent / 2,2,6,6-tetramethyl-1-piperidinyloxy free radical; iodosobenzene diacetate / acetonitrile; H2O / 4 h / 20 °C
2: SOCl2; DMF / CHCl3 / 5 h / Heating

References:

Middleton, Richard J.;Briddon, Stephen J.;Cordeaux, Yolande;Yates, Andrew S.;Dale, Clare L.;George, Michael W.;Baker, Julian G.;Hill, Stephen J.;Kellam, Barrie [Journal of Medicinal Chemistry,2007,vol. 50,# 4,p. 782 - 793]

28440-13-3 Synthesis
2',3'-O-Isopropylideneinosine-5'-carboxylic acid

28440-13-3
13 suppliers
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1-(6-Chloro-9H-purin-9-yl)-1-deoxy-2,3-O-isopropylidene-beta-D-ribofuranuronoyl chloride

104940-65-0
17 suppliers
inquiry

References
58-63-9 Synthesis
Inosine

58-63-9
667 suppliers
$5.00/25g

1-(6-Chloro-9H-purin-9-yl)-1-deoxy-2,3-O-isopropylidene-beta-D-ribofuranuronoyl chloride

104940-65-0
17 suppliers
inquiry

References