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1087792-34-4

methyl 13-oxo-12-oxa-2,3,5,7-tetraazatricyclo[7.4.0.0,2,6]trideca-1(9),3,5,7-tetraene-4-carboxylate synthesis

1synthesis methods
ethyl 2-(4,5-dihydrofuran-3-yl)-2-oxoacetate

96406-00-7
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3641-14-3 Synthesis
Methyl 5-amino-1H-1,2,4-triazole-3-carboxylate

3641-14-3
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$6.00/1g

methyl 13-oxo-12-oxa-2,3,5,7-tetraazatricyclo[7.4.0.0,2,6]trideca-1(9),3,5,7-tetraene-4-carboxylate

1087792-34-4
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Yield:1087792-34-4 68%

Reaction Conditions:

with acetic acid for 36 h;Reflux;regioselective reaction;

References:

Stepaniuk, Oleksandr O.;Matvienko, Vitalii O.;Kondratov, Ivan S.;Shishkin, Oleg V.;Volochnyuk, Dmitriy M.;Mykhailiuk, Pavel K.;Tolmachev, Andrei A. [Synthesis,2012,vol. 44,# 6,p. 895 - 902] Location in patent:experimental part