2-(4-Methyoxyphenyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine synthesis
- Product Name:2-(4-Methyoxyphenyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine
- CAS Number:1159803-53-8
- Molecular formula:C17H15BN2O
- Molecular Weight:274.12
5720-07-0
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Yield:1159803-53-8 95%
Reaction Conditions:
at 150; for 0.25 h;Microwave irradiation;Sealed tube;
Steps:
4.2 General procedures for the synthesis of compounds 5a-f
General procedure: The1,8-diaminonaphthalene (0.4 mmol) and boronic acid (0.4 mmol) were added to a microwave tube and sealed with a microwave septum. The tube was shaken to mix and subjected to microwave irradiation at 150 °C for 15 min (150 W) under a closed system. 1H, 11B and 13C NMR spectra in DMSO-d6 were used to confirm the product obtained by this method was identical to that obtained for Method C.
References:
Slabber, Cathryn A.;Grimmer, Craig D.;Robinson, Ross S. [Journal of Organometallic Chemistry,2013,vol. 723,p. 122 - 128]
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![1H-Naphtho[1,8-de]-1,3,2-diazaborine, 2,3-dihydro-](/CAS/20211123/GIF/5656-71-3.gif)
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