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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
1174130-62-1

(R)-4-(4-((2-(3,5-dimethylphenyl)pyrrolidin-1-yl)methyl)phenoxy)-3-fluorobenzamide synthesis

7synthesis methods
1174130-60-9 Synthesis
4-{4-[2-(3,5-Dimethyl-phenyl)-pyrrolidin-1-ylmethyl]-phenoxy}-3-fluoro-benzamide

1174130-60-9
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(R)-4-(4-((2-(3,5-dimethylphenyl)pyrrolidin-1-yl)methyl)phenoxy)-3-fluorobenzamide

1174130-62-1
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(S)-4-(4-((2-(3,5-diMethylphenyl)pyrrolidin-1-yl)Methyl)phenoxy)-3-fluorobenzaMide

1174130-61-0
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Yield:98 % ee ， 98 % ee

Reaction Conditions:

in 1,2-dimethoxyethane;ethanol;hexane;Purification / work up;Resolution of racemate;

References:

US2009/186873,2009,A1 Location in patent:Page/Page column 6

1174130-60-9 Synthesis
4-{4-[2-(3,5-Dimethyl-phenyl)-pyrrolidin-1-ylmethyl]-phenoxy}-3-fluoro-benzamide

1174130-60-9
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(R)-4-(4-((2-(3,5-dimethylphenyl)pyrrolidin-1-yl)methyl)phenoxy)-3-fluorobenzamide

1174130-62-1
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References
676494-56-7 Synthesis
3-FLUORO-4-(4-FORMYLPHENOXY)BENZAMIDE

676494-56-7
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1213509-59-1 Synthesis
(2R)-2-(3,5-dimethylphenyl)pyrrolidine

1213509-59-1
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(R)-4-(4-((2-(3,5-dimethylphenyl)pyrrolidin-1-yl)methyl)phenoxy)-3-fluorobenzamide

1174130-62-1
2 suppliers
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References
676494-55-6 Synthesis
3-fluoro-4-(4-formylphenoxy)benzonitrile

676494-55-6
28 suppliers
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(R)-4-(4-((2-(3,5-dimethylphenyl)pyrrolidin-1-yl)methyl)phenoxy)-3-fluorobenzamide

1174130-62-1
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References
64248-62-0 Synthesis
3,4-Difluorobenzonitrile

64248-62-0
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(R)-4-(4-((2-(3,5-dimethylphenyl)pyrrolidin-1-yl)methyl)phenoxy)-3-fluorobenzamide

1174130-62-1
2 suppliers
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References