BIS(1,3-DIMETHYLCYCLOPENTADIENYL)ZIRCONIUM DICHLORIDE synthesis
- Product Name:BIS(1,3-DIMETHYLCYCLOPENTADIENYL)ZIRCONIUM DICHLORIDE
- CAS Number:119445-92-0
- Molecular formula:C14H18Cl2Zr10*
- Molecular Weight:348.42
10026-11-6
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Yield:119445-92-0 37%
Reaction Conditions:
with C5H4Me2;BuLi;HCl in hexane;water;toluene;stirring (room temp., 1 h, vac.), ZrCl4 addn., refluxing (Ar-atmosphere), HCl (aq) addn.; filtering, recrystn. (toluene);
References:
Hiller, Jo?rg;Thewalt, Ulf;Pola?s?ek, Miroslav;Petrusova?, Lidmila;Varga, Vojtech;Sedmera, Petr;Mach, Karel [Organometallics,1996,vol. 15,# 17,p. 3752 - 3759]