Adenosine, N-(3-hydroxyphenyl)-, 2',3',5'-triacetate synthesis
- Product Name:Adenosine, N-(3-hydroxyphenyl)-, 2',3',5'-triacetate
- CAS Number:1221412-23-2
- Molecular formula:C22H23N5O8
- Molecular Weight:485.45
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Yield:1221412-23-2 1.51 g
Reaction Conditions:
with triethylamine in ethanol at 60; for 8 h;
Steps:
1.3
Take 5.4g of tri-O-acetyl-6-chloroadenosine and 4.28g of 3-aminophenol, add 30ml of absolute ethanol and 3.96g of triethylamine, and react at 60°C for 8h, then evaporate the solvent under reduced pressure. The residue was purified by silica gel column chromatography, eluent: ethyl acetate: petroleum ether = 2:1, collect the required components, and concentrate under reduced pressure to obtain 2',3',5'-tri-O-acetyl -N6-(3-hydroxyphenyl)adenosine 1.51g.
References:
CN112979734,2021,A Location in patent:Paragraph 0006; 0036; 0039
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