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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List 1H-Pyrazole-1-acetic acid, 4-[5,6-dihydro-2-[3-Methyl-1-(1-Methylethyl)-1H-1,2,4-triazol-5-yl]iMidazo[1,2-d][1,4]benzoxazepin-9-yl]-α,α-diMethyl-, ethyl ester
1282514-64-0

1H-Pyrazole-1-acetic acid, 4-[5,6-dihydro-2-[3-Methyl-1-(1-Methylethyl)-1H-1,2,4-triazol-5-yl]iMidazo[1,2-d][1,4]benzoxazepin-9-yl]-α,α-diMethyl-, ethyl ester synthesis

8synthesis methods
IMidazo[1,2-d][1,4]benzoxazepine, 9-broMo-5,6-dihydro-2-[3-Methyl-1-(1-Methylethyl)-1H-1,2,4-triazol-5-yl]-

1282514-63-9
25 suppliers
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GDC-0032

1282512-48-4
129 suppliers
$32.00/1mg

1H-Pyrazole-1-acetic acid, 4-[5,6-dihydro-2-[3-Methyl-1-(1-Methylethyl)-1H-1,2,4-triazol-5-yl]iMidazo[1,2-d][1,4]benzoxazepin-9-yl]-α,α-diMethyl-, ethyl ester

1282514-64-0
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-

Yield:-

Reaction Conditions:

with chloro(2-dicyclohexylphosphino-2’,4’,6’-triisopropyl-1,1‘-biphenyl)[2-(2’-amino-1,1‘-biphenyl’)]palladium(II);potassium acetate;lithium hydroxide;XPhos in tetrahydrofuran;ethanol;water at 77;Large scale;Suzuki-Miyaura Coupling;

References:

St-Jean, Frédéric;Remarchuk, Travis;Angelaud, Rémy;Carrera, Diane E.;Beaudry, Danial;Malhotra, Sushant;McClory, Andrew;Kumar, Archana;Ohlenbusch, Gerd;Schuster, Andreas M.;Gosselin, Francis [Organic Process Research and Development,2019,vol. 23,# 5,p. 783 - 793]

600-00-0 Synthesis
Ethyl 2-bromoisobutyrate

600-00-0
270 suppliers
$13.00/5g

1H-Pyrazole-1-acetic acid, 4-[5,6-dihydro-2-[3-Methyl-1-(1-Methylethyl)-1H-1,2,4-triazol-5-yl]iMidazo[1,2-d][1,4]benzoxazepin-9-yl]-α,α-diMethyl-, ethyl ester

1282514-64-0
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References
105942-08-3 Synthesis
4-Bromo-2-fluorobenzonitrile

105942-08-3
381 suppliers
$7.00/5g

1H-Pyrazole-1-acetic acid, 4-[5,6-dihydro-2-[3-Methyl-1-(1-Methylethyl)-1H-1,2,4-triazol-5-yl]iMidazo[1,2-d][1,4]benzoxazepin-9-yl]-α,α-diMethyl-, ethyl ester

1282514-64-0
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References
635702-31-7 Synthesis
4-BROMO-2-FLUORO-N-HYDROXYBENZAMIDINE

635702-31-7
16 suppliers
$78.29/1g

1H-Pyrazole-1-acetic acid, 4-[5,6-dihydro-2-[3-Methyl-1-(1-Methylethyl)-1H-1,2,4-triazol-5-yl]iMidazo[1,2-d][1,4]benzoxazepin-9-yl]-α,α-diMethyl-, ethyl ester

1282514-64-0
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References
9-bromo-5,6-dihydrobenzo[f]imidazo[1,2-d][1,4]oxazepine-2-carboxylicacid

1282516-74-8
12 suppliers
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1H-Pyrazole-1-acetic acid, 4-[5,6-dihydro-2-[3-Methyl-1-(1-Methylethyl)-1H-1,2,4-triazol-5-yl]iMidazo[1,2-d][1,4]benzoxazepin-9-yl]-α,α-diMethyl-, ethyl ester

1282514-64-0
12 suppliers
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References