7-PHENYL-TRICYCLO[4.1.0.0(2,7)]HEPTANE-1-CARBOXYLIC ACID synthesis

2synthesis methods

Product Name:7-PHENYL-TRICYCLO[4.1.0.0(2,7)]HEPTANE-1-CARBOXYLIC ACID
CAS Number:129576-92-7
Molecular formula:C14H14O2
Molecular Weight:214.26

Bicyclo[4.1.0]heptane, 7,7-dibromo-1-phenyl-

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7-PHENYL-TRICYCLO[4.1.0.0(2,7)]HEPTANE-1-CARBOXYLIC ACID

129576-92-7
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$45.00/10mg

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 80 percent / methyllithium / pentane; diethyl ether / 2 h / Ambient temperature
2: 1.) butyllithium, tetramethylenediamine / 1.) pentane, RT, 4 h, 2.) pentane, diethyl ether, from -30 deg C to RT

References:

Koptelov, Yu. B.;Kostikov, R. R.;Molchanov, A. P. [Journal of Organic Chemistry USSR (English Translation),1990,vol. 26,# 12,p. 2181 - 2185][Zhurnal Organicheskoi Khimii,1990,vol. 26,# 12,p. 2518 - 2523]

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129576-92-7
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$45.00/10mg

References