(S)-(2-Amino-1-phenyl-ethyl)-carbamic acid benzyl ester synthesis
- Product Name:(S)-(2-Amino-1-phenyl-ethyl)-carbamic acid benzyl ester
- CAS Number:130406-36-9
- Molecular formula:C16H18N2O2
- Molecular Weight:270.33
![Carbamic acid, [(1S)-2-azido-1-phenylethyl]-, phenylmethyl ester (9CI)](/CAS/20211123/GIF/190393-65-8.gif)
190393-65-8
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130406-36-9
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Yield:130406-36-9 87%
Reaction Conditions:
Stage #1: (S)-2-<(benzyloxycarbonyl)amino>-2-phenyl ethyl azidewith triphenylphosphine in tetrahydrofuran; for 8 h;Reflux;
Stage #2: with water in tetrahydrofuran; for 16 h;Reflux;
References:
Fotaras, Stamatis;Kokotos, Christoforos G.;Kokotos, George [Organic and Biomolecular Chemistry,2012,vol. 10,# 29,p. 5613 - 5619] Location in patent:supporting information; experimental part
130406-31-4
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130406-36-9
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20989-17-7
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130406-36-9
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501-53-1
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117049-14-6
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130406-36-9
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