4-(4-(Prop-2-yn-1-yloxy)phenyl)-1,2,4-triazolidine-3,5-dione synthesis
- Product Name:4-(4-(Prop-2-yn-1-yloxy)phenyl)-1,2,4-triazolidine-3,5-dione
- CAS Number:1313211-51-6
- Molecular formula:C11H9N3O3
- Molecular Weight:231.21
26557-78-8
56 suppliers
$75.00/50mg
4114-31-2
248 suppliers
$5.00/10g
1313211-51-6
9 suppliers
$424.00/500mg
Yield:1313211-51-6 47%
Reaction Conditions:
Stage #1: ethylhydrazine carboxylatewith 1,1'-carbonyldiimidazole in tetrahydrofuran at 23; for 2 h;
Stage #2: 4-(prop-2-ynyloxy)anilinewith triethylamine in tetrahydrofuran at 45; for 3 h;
References:
Naik, Anu;Alzeer, Jawad;Triemer, Therese;Bujalska, Anna;Luedtke, Nathan W. [Angewandte Chemie - International Edition,2017,vol. 56,# 36,p. 10850 - 10853][Angew. Chem.,2017,vol. 129,# 36,p. 10990 - 10993,4] Location in patent:supporting information
26557-78-8
56 suppliers
$75.00/50mg
1313211-51-6
9 suppliers
$424.00/500mg
54840-15-2
110 suppliers
$8.00/1g
1313211-51-6
9 suppliers
$424.00/500mg
54840-30-1
11 suppliers
$1052.00/5g
1313211-51-6
9 suppliers
$424.00/500mg
100-02-7
61 suppliers
$11.00/5G
1313211-51-6
9 suppliers
$424.00/500mg