TERT-BUTYL (2-BROMO-5-FORMYL-1H-PYRROL-1-YL)CARBAMATE synthesis
- Product Name:TERT-BUTYL (2-BROMO-5-FORMYL-1H-PYRROL-1-YL)CARBAMATE
- CAS Number:1318629-68-3
- Molecular formula:C10H13BrN2O3
- Molecular Weight:289.13
937046-95-2
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione / tetrahydrofuran; 1-methyl-pyrrolidin-2-one / 1 - 6 °C / Inert atmosphere; Darkness
2.1: TurboGrignard / tetrahydrofuran; 1,4-dioxane / 9 - 23 °C / Inert atmosphere
2.2: 3 - 23 °C / Inert atmosphere
References:
Thieu, Tho;Sclafani, Joseph A.;Levy, Daniel V.;McLean, Andrew;Breslin, Henry J.;Ott, Gregory R.;Bakale, Roger P.;Dorsey, Bruce D. [Organic Letters,2011,vol. 13,# 16,p. 4204 - 4207]
870-46-2
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