dimethyl 5'-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-[1,1':3',1''-terphenyl]-4,4''-dicarboxylate synthesis
- Product Name:dimethyl 5'-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-[1,1':3',1''-terphenyl]-4,4''-dicarboxylate
- CAS Number:1331745-91-5
- Molecular formula:C28H29BO6
- Molecular Weight:472.34
626-39-1
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1331745-91-5
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; methanol; water / 36 h / Inert atmosphere; Reflux
2: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,2-dimethoxyethane / 3 h / Inert atmosphere; Reflux
References:
Gole, Bappaditya;Bar, Arun Kumar;Mallick, Arijit;Banerjee, Rahul;Mukherjee, Partha Sarathi [Chemical Communications,2013,vol. 49,# 67,p. 7439 - 7441]
195062-62-5
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89280-77-3
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$181.00/500mg
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106-40-1
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$12.00/5g
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28165-52-8
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$8.00/250mg
1331745-91-5
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