2-(Adamantan-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane synthesis
- Product Name:2-(Adamantan-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
- CAS Number:1357000-33-9
- Molecular formula:C16H27BO2
- Molecular Weight:262.2
76-09-5
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768-93-4
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$171.00/5g
13826-27-2
142 suppliers
$5.00/250mg
1357000-33-9
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Yield:1357000-33-9 97%
Reaction Conditions:
Stage #1: 1-iodoadamantane;2,2'-bis(1,3,2-benzodioxaborole)with tetrabutylammonium tetrafluoroborate in N,N-dimethyl-formamide at 25; for 0.2 h;Electrolysis;Inert atmosphere;
Stage #2: 2,3-dimethyl-2,3-butane diolwith triethylamine in N,N-dimethyl-formamide at 25; for 1 h;Inert atmosphere;
References:
Wang, Bingbing;Peng, Pan;Ma, Wan;Liu, Zhao;Huang, Cheng;Cao, Yangmin;Hu, Ping;Qi, Xiaotian;Lu, Qingquan [Journal of the American Chemical Society,2021,vol. 143,# 33,p. 12985 - 12991] Location in patent:supporting information
768-90-1
418 suppliers
$10.00/5g
76-09-5
400 suppliers
$10.00/1g
13826-27-2
142 suppliers
$5.00/250mg
1357000-33-9
8 suppliers
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768-90-1
418 suppliers
$10.00/5g
76-09-5
400 suppliers
$10.00/1g
274-07-7
168 suppliers
$78.09/5g
1357000-33-9
8 suppliers
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76-09-5
400 suppliers
$10.00/1g
13826-27-2
142 suppliers
$5.00/250mg
![Tricyclo[3.3.1.13,7]decane-1-carboxylic acid, 1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl ester](/CAS/20210111/GIF/118334-83-1.gif)
118334-83-1
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1357000-33-9
8 suppliers
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