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135711-62-5

(1α,3R,4α,5R)-3,5-Bis[[(1,1-diMethylethyl)diMethylsilyl]oxy]-1,4-dihydroxy-cyclohexanecarboxylic Acid Methyl Ester synthesis

2synthesis methods
Cyclohexanecarboxylic acid, 1,3,4,5-tetrahydroxy-, methyl ester, (1α,3R,4α,5R)-

191916-39-9
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18162-48-6 Synthesis
tert-Butyldimethylsilyl chloride

18162-48-6
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$9.00/5g

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Yield:135711-62-5 75%

Reaction Conditions:

with triethylamine in N,N-dimethyl-formamide at 0 - 20; for 18 h;

References:

Sanchez-Abella, Laura;Fernandez, Susana;Armesto, Nuria;Ferrero, Miguel;Gotor, Vicente [Journal of Organic Chemistry,2006,vol. 71,# 14,p. 5396 - 5399]