methyl 1-(6-bromonaphthalen-2-yl)cyclopropane-1-carboxylate synthesis
- Product Name:methyl 1-(6-bromonaphthalen-2-yl)cyclopropane-1-carboxylate
- CAS Number:1423703-16-5
- Molecular formula:C15H13BrO2
- Molecular Weight:305.17
33626-98-1
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Yield:-
Steps:
Multi-step reaction with 6 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 0 - 20 °C
2.1: thionyl chloride; zinc(II) chloride / dichloromethane / -5 - 20 °C
3.1: acetonitrile / Reflux
4.1: sodium hydride / dimethyl sulfoxide / 2 h / 0 - 20 °C
5.1: sodium hydroxide; ethylene glycol / 72 h / 150 °C / Sealed tube
5.2: pH 2
6.1: hydrogenchloride / 3 h / Reflux
References:
WO2013/25733,2013,A1
100751-63-1
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