TERT-BUTYL 2-(TERT-BUTOXYCARBONYLAMINO)HEX-5-ENOATE synthesis
- Product Name:TERT-BUTYL 2-(TERT-BUTOXYCARBONYLAMINO)HEX-5-ENOATE
- CAS Number:151294-93-8
- Molecular formula:C15H27NO4
- Molecular Weight:285.38
5162-44-7
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111652-20-1
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151294-93-8
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Yield:151294-93-8 86%
Reaction Conditions:
Stage #1: N-(tert-butoxycarbonyl)glycine tert-butyl esterwith N,N,N,N,N,N-hexamethylphosphoric triamide;n-butyllithium in tetrahydrofuran at -78;Metallation;
Stage #2: 1-bromo-4-butene in tetrahydrofuran at -78 - 20; for 7.5 h;Alkylation;
References:
Adamczyk, Maciej;Johnson, Donald D.;Reddy, Rajarathnam E. [Tetrahedron,1999,vol. 55,# 1,p. 63 - 88]
![L-Norvaline, N-[(1,1-dimethylethoxy)carbonyl]-5-oxo-, 1,1-dimethylethyl ester](/CAS/GIF/194656-73-0.gif)
16258-05-2
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151294-93-8
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122471-00-5
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151294-93-8
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