3'-O-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-Thymidine synthesis
- Product Name:3'-O-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-Thymidine
- CAS Number:161322-80-1
- Molecular formula:C18H17N3O7
- Molecular Weight:387.34
50-89-5
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: triethylamine; dmap / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere
2.1: triethylamine; methanesulfonyl chloride / 2 h / 20 °C / Inert atmosphere
2.2: 1.5 h / Inert atmosphere; Reflux
3.1: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 2 h / 0 - 20 °C / Inert atmosphere
4.1: acetic acid / 3 h / 20 °C / Inert atmosphere
References:
De, Swarup;Groaz, Elisabetta;Herdewijn, Piet [European Journal of Organic Chemistry,2014,vol. 2014,# 11,p. 2322 - 2348]
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