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ChemicalBook CAS DataBase List 2-Amino-6-chloro-9H-purine-9-acetic acid benzyl ester
169287-67-6

2-Amino-6-chloro-9H-purine-9-acetic acid benzyl ester synthesis

2synthesis methods
-

Yield:169287-67-6 89%

Reaction Conditions:

Stage #1: 2-Amino-6-chloropurin;Benzyl bromoacetatewith potassium carbonate in N,N-dimethyl-formamide at 0 - 23;Inert atmosphere;
Stage #2: Inert atmosphere;

References:

Pothukanuri, Srinivasu;Pianowski, Zbigniew;Winssinger, Nicolas [European Journal of Organic Chemistry,2008,# 18,p. 3141 - 3148] Location in patent:supporting information; experimental part