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ChemicalBook CAS DataBase List N2-iso-Butyroyl-5'-(4,4'-dimethoxytrityl)-2'-O-propargylguanosine
171486-53-6

N2-iso-Butyroyl-5'-(4,4'-dimethoxytrityl)-2'-O-propargylguanosine synthesis

2synthesis methods
-

Yield:171486-53-6 55% ,171486-57-0 22%

Reaction Conditions:

with tetra-(n-butyl)ammonium iodide;di(n-butyl)tin oxide in acetonitrile;benzene at 100;Inert atmosphere;Microwave irradiation;Sealed bottle;

References:

Yamada, Takeshi;Peng, Chang Geng;Matsuda, Shigeo;Addepalli, Haripriya;Jayaprakash, K. Narayanannair;Alam, Md. Rowshon;Mills, Kathy;Maier, Martin A.;Charisse, Klaus;Sekine, Mitsuo;Manoharan, Muthiah;Rajeev, Kallanthottathil G. [Journal of Organic Chemistry,2011,vol. 76,# 5,p. 1198 - 1211] Location in patent:supporting information; experimental part