4-Acetyl-3-methyl-5-(methylthio)thiophene-2-carbonitrile synthesis
- Product Name:4-Acetyl-3-methyl-5-(methylthio)thiophene-2-carbonitrile
- CAS Number:175202-62-7
- Molecular formula:C9H9NOS2
- Molecular Weight:211.3
![3-[Bis(methylsulfanyl)methylene]-2,4-pentanedione](/CAS/GIF/15908-50-6.gif)
15908-50-6
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$265.00/100mg
107-14-2
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175202-62-7
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Yield:175202-62-7 37%
Reaction Conditions:
Stage #1: 3-[di(methylthio)methylene]pentane-2,4-dionewith sodium sulfide in N,N-dimethyl-formamide at 50; for 1 h;
Stage #2: chloroacetonitrilewith potassium carbonate in N,N-dimethyl-formamide at 50; for 6 h;
References:
Sommen, Geoffroy;Comel, Alain;Kirsch, Gilbert [Synthesis,2003,# 5,p. 735 - 741]
107-14-2
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$15.00/25g
123-54-6
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$10.00/25ml
74-88-4
327 suppliers
$15.00/10g
175202-62-7
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