Ethyl 2-(8-hydroxy-1,4-dioxaspiro[4.5]decan-8-yl)acetate synthesis

1synthesis methods

4746-97-8 Synthesis

105-36-2 Synthesis

Yield:189509-22-6 93%

Reaction Conditions:

with zinc in tetrahydrofuran; for 8 h;Heating;Reformatzky reaction;

References:

Liang, Pi-Hui;Hsin, Ling-Wei;Pong, Sung-Ling;Hsu, Chia-Huei;Cheng, Chen-Yu [Journal of the Chinese Chemical Society,2003,vol. 50,# 3 A,p. 449 - 456]

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