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ChemicalBook CAS DataBase List 1H-Indene-2-carboxamide,2,3-dihydro-(9CI)

1H-Indene-2-carboxamide,2,3-dihydro-(9CI) synthesis

6synthesis methods
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Yield:175079-50-2 73%

Reaction Conditions:

Stage #1: indan-2-ol;sodium cyanidewith chloro-trimethyl-silane;sodium iodide in N,N-dimethyl-formamide;acetonitrile at 60; for 5 h;Substitution;
Stage #2: with sodium hypochlorite;waterHydrolysis;

References:

Bowers, Nigel I.;Boyd, Derek R.;Sharma, Narain D.;Goodrich, Peter A.;Groocock, Melanie R.;Blacker, A. John;Goode, Paul;Dalton, Howard [Journal of the Chemical Society. Perkin transactions I,1999,# 11,p. 1453 - 1461]

26453-01-0 Synthesis
2,3-Dihydro-1H-indene-2-carbonitrile

26453-01-0
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1H-Indene-2-carboxamide,2,3-dihydro-(9CI)

175079-50-2
3 suppliers
inquiry