1H-Indole, 1-hydroxy- synthesis
- Product Name:1H-Indole, 1-hydroxy-
- CAS Number:3289-82-5
- Molecular formula:C8H7NO
- Molecular Weight:133.15
120-72-9
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Yield:3289-82-5 96%
Reaction Conditions:
with 2-hydroxy-N,N,N-trimethyl ethanaminium peroxydisulfate at 60; for 1 h;Inert atmosphere;Green chemistry;chemoselective reaction;
Steps:
N,N-Disubstituted Hydroxylamines 1a-m; General Procedure
General procedure: A round-bottomed flask was charged with the secondary amine(5 mmol) and ChPS (5.5 mmol) and the mixture was stirred for1 h at 60 °C under N2. The mixture was then dissolved in H2O (5 mL) and the product was extracted with CH2Cl2 or EtOAc (3 × 5mL). The combined organic layers were dried (Na2SO4), filtered,and concentrated under reduced pressure.
References:
Banan, Alireza;Valizadeh, Hassan;Heydari, Akbar;Moghimi, Abolghasem [Synlett,2017,vol. 28,# 17,art. no. ST-2017-D0281-L,p. 2315 - 2319]
496-15-1
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20973-67-5
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86531-02-4
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3289-82-5
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1969-73-9
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120-72-9
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3289-82-5
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88-72-2
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95-53-4
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