ChemicalBook CAS DataBase List (1S)-1-(4-FLUOROPHENYL)BUT-3-EN-1-AMINE

(1S)-1-(4-FLUOROPHENYL)BUT-3-EN-1-AMINE synthesis

2synthesis methods

Product Name:(1S)-1-(4-FLUOROPHENYL)BUT-3-EN-1-AMINE
CAS Number:949096-30-4
Molecular formula:C10H12FN
Molecular Weight:165.2074

Benzoic acid, 2-[(4-fluorophenyl)methylene]hydrazide

115504-61-5
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: C₃₄H₃₂N₂O₂*F₆P^(1-)*H⁽¹⁺⁾ / methanol / 1 h / 20 °C / Inert atmosphere
1.2: 12 h / 20 °C / Inert atmosphere
1.3: Inert atmosphere
2.1: methanol; samarium diiodide / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

References:

Piao, Fengnu;Mishra, Mithilesh Kumar;Jang, Doo Ok [Tetrahedron,2012,vol. 68,# 35,p. 7050 - 7055]

459-57-4 Synthesis

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References

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