2,2,3-Trimethyl-3-butenoic acid synthesis

12synthesis methods

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 86 percent / POCl₃, pyridine / 5 h / Ambient temperature
2: 81 percent / aq. KOH / ethanol / 2 h / Heating

References:

Fraenkel, Gideon;Duncan, Joseph H.;Wang, Jinhai [Journal of the American Chemical Society,1999,vol. 121,# 2,p. 432 - 443]

563-79-1 Synthesis

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