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ChemicalBook CAS DataBase List (2-(2-chloroethoxy)-5-nitrophenyl)Methanol
937273-30-8

(2-(2-chloroethoxy)-5-nitrophenyl)Methanol synthesis

3synthesis methods
110837-53-1 Synthesis
2-(2-chloroethoxy)-5-nitrobenzaldehyde

110837-53-1
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(2-(2-chloroethoxy)-5-nitrophenyl)Methanol

937273-30-8
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Yield:937273-30-8 100%

Reaction Conditions:

with sodium tetrahydroborate in tetrahydrofuran at 0 - 20;

References:

William, Anthony D.;Lee, Angeline C.-H.;Blanchard, Stéphanie;Poulsen, Anders;Teo, Ee Ling;Nagaraj, Harish;Tan, Evelyn;Chen, Dizhong;Williams, Meredith;Sun, Eric T.;Goh, Kee Chuan;Ong, Wai Chung;Goh, Siok Kun;Hart, Stefan;Jayaraman, Ramesh;Pasha, Mohammed Khalid;Ethirajulu, Kantharaj;Wood, Jeanette M.;Dymock, Brian W. [Journal of Medicinal Chemistry,2011,vol. 54,# 13,p. 4638 - 4658] Location in patent:experimental part