2-(2-CHLOROPHENYLSULFANYL)BENZOTHIAZOLE synthesis
- Product Name:2-(2-CHLOROPHENYLSULFANYL)BENZOTHIAZOLE
- CAS Number:60372-34-1
- Molecular formula:C13H8ClNS2
- Molecular Weight:277.79
Yield:60372-34-1 213 mg
Reaction Conditions:
Stage #1: 2-Mercaptobenzothiazolewith 1,10-Phenanthroline;potassium carbonate;copper(I) bromide in water at 80; for 15 h;
Stage #2: 2-iodochlorobenzenewith 1,10-Phenanthroline;potassium carbonate;copper(I) bromide in water at 80; for 15 h;
References:
Liu, Xing;Zhang, Shi-Bo;Zhu, Hui;Dong, Zhi-Bing [Journal of Organic Chemistry,2018,vol. 83,# 19,p. 11703 - 11711]
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