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ChemicalBook CAS DataBase List (2,2-DIMETHYL-[1,3]-DIOXOLAN-4-YL)-METHYLAMINE
22195-47-7

(2,2-DIMETHYL-[1,3]-DIOXOLAN-4-YL)-METHYLAMINE synthesis

11synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: LiAlH4 / tetrahydrofuran / 2 h / Heating
2: aq. NaIO4 / tetrahydrofuran / 2 h / 0 °C
3: NH2OH*HCl, Et3N / tetrahydrofuran; methanol / 5 h / 10 °C
4: LiAlH4 / tetrahydrofuran / 5 h / Ambient temperature

References:

Danielmeier, Karsten;Steckhan, Eberhard [Tetrahedron Asymmetry,1995,vol. 6,# 5,p. 1181 - 1190]

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